Chemistry Senior 4

Complete Study Guide · Units 5 to 10

Rwanda Education Board Curriculum

Quick Navigation

5 Periodic Trends — Physical 6 Group 1 — Alkali Metals 7 Group 2 — Alkaline Earths 8 Group 13 — Boron Group 9 Group 14 — Carbon Group 10 Group 15 — Nitrogen Group
5
Variation in Trends of Physical Properties
Key competency: Use atomic structure to explain trends in physical properties

The Periodic Table — Brief History

The modern periodic table is the result of more than a century of scientific work. Here are the most important milestones to know:

ScientistYearContribution
Döbereiner1829Law of Triads — middle element's properties average those of the other two in a group of three similar elements
Newlands1863Law of Octaves — every 8th element has similar properties (failed beyond Calcium)
Mendeleev1869Arranged ~66 elements by increasing atomic mass; left gaps for undiscovered elements; predicted their properties
Moseley1913Rearranged elements by atomic number — this is the basis of the modern table
Seaborg1944Discovered 10 new elements; separated the actinide series (placed below main body)
Key factThe modern periodic table has 118 elements, arranged in 18 groups (columns) and 7 periods (rows), ordered by increasing atomic number.

Locating Elements — Groups, Periods & Blocks

Finding the Period

The period number = the highest principal quantum number (n) occupied by electrons.

ExampleSulphur: 1s²2s²2p⁶3s²3p⁴ → highest n = 3 → Period 3

Finding the Group

Count valence electrons in the outermost sub-shell(s):

Last sub-shellGroup
ns¹1
ns²2
ns²np¹ to ns²np⁶13 to 18
ns² + (n-1)d¹⁻¹⁰ (transition)3 to 12 (add both)

The Four Blocks

s-block (Groups 1 & 2)Last electron in s orbital. Reactive metals, low IE, lose electrons easily to form +1 or +2 ions.
p-block (Groups 13–18)Last electron in p orbital. Mix of metals, non-metals and metalloids. Form mostly covalent compounds.
d-block (Groups 3–12)Transition metals. Variable oxidation states, form coloured ions, good catalysts.
f-block (below main table)Lanthanides (Ce–Lu) and actinides (Th–Lr). All metals. Many actinides are radioactive.

Trends in Physical Properties

1. Atomic Radius

Across a period →Atomic radius decreases. More protons pull electrons closer to nucleus (same energy level, but stronger pull).
Down a group ↓Atomic radius increases. New electron shells added → electrons farther from nucleus.

2. Electronegativity

Across a period →Electronegativity increases. More protons attract bonding pairs more strongly.
Down a group ↓Electronegativity decreases. Larger atomic radius; nucleus too far to attract external electrons strongly. Most electronegative = Fluorine; Least = Francium.

3. Ionisation Energy (IE)

IE = energy needed to remove an electron from a neutral gaseous atom. The key rule: 1st IE < 2nd IE < 3rd IE (each successive electron is harder to remove because the remaining electrons are more tightly held).

Across a period →IE increases. Greater nuclear charge holds outer electrons more tightly.
Down a group ↓IE decreases. Outer electrons farther from nucleus, shielded by inner shells.
Exception to knowN has HIGHER 1st IE than O (same period). Nitrogen has a half-filled 2p³ which is extra stable. Removing an electron from O's paired 2p is actually easier.

4. Melting & Boiling Points

In the left (metallic) region of the periodic table: melting points decrease down a group (weaker metallic bonding). In the right (non-metal) region (groups 17, 18): melting points increase down a group (larger molecules → stronger van der Waals forces).

5. Density

Generally increases down a group (mass increases faster than volume). In a period, density peaks in the middle (d-block) where atomic mass is high and atomic radius is relatively small.

6. Metallic Character & Electron Affinity

Metallic character increases down a group and decreases across a period (left to right).
Electron affinity generally increases across a period (nucleus attracts an extra electron more) and decreases down a group (larger radius → weaker attraction).
🧠 Quick Memory Summary for Unit 5
Going right across a period: radius ↓, EN ↑, IE ↑, metallic ↓.
Going down a group: radius ↑, EN ↓, IE ↓, metallic ↑.
6
Group 1 Elements & Their Compounds (Alkali Metals)
Key competency: Compare chemical properties of Group 1 elements relative to their position in the periodic table

Who Are They?

Li (Lithium)Na (Sodium)K (Potassium)Rb (Rubidium)Cs (Caesium)Fr (Francium)

All Group 1 elements have the valence electronic configuration ns¹. They are soft, silvery metals that are stored in oil to prevent reaction with air and moisture. Hydrogen has the same ns¹ configuration but is NOT a Group 1 metal — it is a gas, non-metal in many compounds, and is studied separately.

Physical Properties Trend (down the group)

PropertyTrend ↓Reason
Atomic radiusIncreasesMore electron shells added
Melting/Boiling pointDecreasesMetallic bond weakens (larger atom, less attractive force between nucleus and electrons)
1st Ionisation EnergyDecreasesValence electron is farther from nucleus; easier to remove
ReactivityIncreasesEasier to lose that one valence electron
DensityGenerally increasesMass increases faster than volume; Li, Na, K are less dense than water

Reactions — the Core Chemistry

With Oxygen (air)

Reactivity increases down the group. The type of oxide formed changes:

4Li + O₂ → 2Li₂O (normal oxide, O²⁻ ion) 2Na + O₂ → Na₂O₂ (peroxide, O₂²⁻ ion) K/Rb/Cs + O₂ → MO₂ (superoxide, O₂⁻ ion)

All oxides dissolve in water to form strongly alkaline (basic) solutions: M₂O + H₂O → 2MOH

With Water

2M(s) + 2H₂O(l) → 2MOH(aq) + H₂(g)

This is why they are called "alkali metals" — they produce alkaline hydroxide solutions with water. Reactivity: Li (slow fizz) < Na (vigorous, hissing) < K (ignites) < Rb < Cs (explosive).

With Halogens

2M(s) + X₂ → 2MX(s) (metal halide salt)

All Group 1 metals react vigorously with halogens to form ionic halides. Reactivity increases down the group.

Anomalous Behaviour of Lithium

Lithium is the smallest Group 1 atom. Its high charge density (charge/size ratio) gives it more covalent character in its compounds. Key differences:

  • Li₂O (normal oxide) — not peroxide like Na
  • Li₂CO₃ decomposes on heating (unlike Na₂CO₃ which is stable)
  • LiNO₃ decomposes like Mg(NO₃)₂ (gives Li₂O + NO₂ + O₂), not LiNO₂ + O₂
  • LiOH and Li₂CO₃ are less soluble than other Group 1 counterparts
  • Li resembles Mg — this is the diagonal relationship

Oxides & Hydroxides

Oxides: All Group 1 oxides are basic. They dissolve in water to form the corresponding hydroxide (MOH).

Hydroxides: All Group 1 hydroxides are strong bases. They dissolve readily in water. Solubility increases down the group (LiOH least soluble → CsOH most soluble).

Effect of Heat on Nitrates & Carbonates

Nitrates (except Li) 2MNO₃ → 2MNO₂ + O₂
Sodium → Caesium all give nitrite + O₂ on heating.
Lithium Nitrate (exception) 2LiNO₃ → Li₂O + 2NO₂ + ½O₂
(Behaves like Group 2 nitrates)
Carbonates (except Li) Na₂CO₃, K₂CO₃ etc. are stable to heat — they do NOT decompose at Bunsen burner temperature.
Lithium Carbonate (exception) Li₂CO₃ → Li₂O + CO₂
(Behaves like Group 2 carbonates)

Solubility Trends

Compound typeTrend down Group 1
Hydroxides (MOH)Solubility increases
Carbonates (M₂CO₃)Solubility increases
Sulphates (M₂SO₄)Solubility decreases

Flame Tests

ElementFlame Colour
Lithium (Li)Deep Red / Crimson
Sodium (Na)Bright Yellow / Orange
Potassium (K)Lilac / Violet
Rubidium (Rb)Red
Caesium (Cs)Blue
How it worksHeat promotes valence electrons to higher energy levels. As they fall back, energy is released as visible light of a specific wavelength (colour).

Important Uses

Lithium: Batteries (phones, pacemakers), Li₂CO₃ to toughen glass, alloys for aircraft.

Sodium: NaOH (caustic soda) in soap/paper making; NaCl for seasoning and manufacturing; Na vapour lamps for street lighting; molten Na as coolant in nuclear reactors.

🧠 The Big Picture for Unit 6
Down Group 1: bigger atom → weaker hold on valence electron → more reactive → lower melting point → lower IE. Li behaves differently because it's tiny (like Mg — diagonal relationship).
7
Group 2 Elements & Their Compounds (Alkaline Earth Metals)
Key competency: Compare properties of Group 2 elements relative to their position in the periodic table

Who Are They?

Be (Beryllium)Mg (Magnesium)Ca (Calcium)Sr (Strontium)Ba (Barium)Ra (Radium)

Valence configuration: ns². All are solid metals at room temperature. They lose 2 electrons to form M²⁺ ions. Called "alkaline earth metals" because their oxides dissolve in water to give alkaline solutions, and were historically called "earths" (they were found in Earth's crust).

Physical Properties Trend

PropertyTrend ↓ the groupReason
Atomic radiusIncreasesExtra electron shells added
Melting/Boiling pointDecreases (generally)Metallic bond weakens with larger atomic radius
1st Ionisation EnergyDecreasesLarger atom; outer electrons farther from nucleus
ReactivityIncreasesEasier to lose 2 electrons as radius grows
ElectronegativityDecreasesLarger radius → less ability to attract electrons

Reactions with Common Substances

ReactantProductNotes
Cold waterM(OH)₂ + H₂Be: no reaction. Mg: no reaction. Ca → Ba: increasingly vigorous
SteamMO + H₂Mg reacts with steam: Mg + H₂O(g) → MgO + H₂
OxygenMO (mostly)Ba forms BaO₂ (peroxide) in excess O₂
Halogens (e.g. Cl₂)MCl₂All react to form ionic halides except BeCl₂ (covalent)
Dilute HClMCl₂ + H₂All react to form the chloride salt + hydrogen gas
NitrogenM₃N₂Requires extremely high temperature

Properties of Compounds

Oxides

Group 2 oxides are basic (ionic). They react with water: MO + H₂O → M(OH)₂. Exception: BeO is amphoteric — it reacts with both acids and bases.

Hydroxides — Solubility Trend

Hydroxides — solubility INCREASES down the group Be(OH)₂ and Mg(OH)₂ → insoluble | Ca(OH)₂ and Sr(OH)₂ → slightly soluble | Ba(OH)₂ → fairly soluble

Sulphates — Opposite trend!

Sulphates — solubility DECREASES down the group BeSO₄ and MgSO₄ → soluble | CaSO₄ → slightly soluble | SrSO₄ and BaSO₄ → insoluble

Carbonates

Sparingly soluble, and their solubility decreases slightly down the group.

Thermal Stability of Carbonates, Hydroxides & Nitrates

MCO₃(s) + heat → MO(s) + CO₂(g) M(OH)₂(s) + heat → MO(s) + H₂O(g) M(NO₃)₂(s) + heat → MO(s) + 2NO₂(g) + ½O₂(g)

Thermal stability increases down the group. Compounds of smaller ions (top of group) have more covalent character and decompose more easily. BeCO₃ decomposes most easily; BaCO₃ is the most stable.

Anomalous Behaviour of Beryllium

Be is unique because its Be²⁺ ion is very small and highly charged → high polarising power → more covalent character than expected.

Be(OH)₂ is amphoteric
As base: Be(OH)₂ + 2H⁺ → Be²⁺ + 2H₂O
As acid: Be(OH)₂ + 2OH⁻ → [Be(OH)₄]²⁻
BeCl₂ is covalent
Dissolves in non-polar organic solvents (unlike other Group 2 chlorides which are ionic). Hydrolyses in water to form Be(OH)₂ + HCl.

Flame Tests for Group 2

ElementFlame Colour
Beryllium / MagnesiumColourless / Bright White
CalciumBrick Red
StrontiumCrimson Red
BariumApple Green

Test for Ba²⁺ ions

Add SO₄²⁻ ions (e.g. Na₂SO₄ solution): a white precipitate of BaSO₄ forms, insoluble even in acid.

Ba²⁺(aq) + SO₄²⁻(aq) → BaSO₄(s) (white precipitate)

Important Uses & Limestone Chemistry

The Limestone Cycle (very important!)
CaCO₃ (limestone) →heat ~1000°C→ CaO (quicklime) + CO₂
CaO + H₂O → Ca(OH)₂ (slaked lime / ishwagara)
Ca(OH)₂ is used to reduce soil acidity, in cement making, and as a cheap base in industry.

Cement: Made by strongly heating limestone + clay → "clinker" → mixed with gypsum (CaSO₄·2H₂O).

Other uses: Mg in chlorophyll (photosynthesis); Mg(OH)₂ as antacid medicine; Ca in bones/teeth; Ba compounds in X-ray contrast agents.

🧠 The Big Contrast: Group 1 vs Group 2
Group 2 is LESS reactive than Group 1 (need to remove 2 electrons, not 1). Group 2 compounds are generally LESS soluble and LESS thermally stable than Group 1 equivalents. Be always behaves differently (more covalent, amphoteric).
8
Group 13 Elements & Their Compounds (Boron Group)
Key competency: Compare chemical properties of Group 13 elements relative to their position in the periodic table

Who Are They?

B (Boron)Al (Aluminium)Ga (Gallium)In (Indium)Tl (Thallium)

Valence configuration: ns²np¹. These are the first p-block elements. Except for Boron, they are all metals. Boron is a non-metal with very high melting point and low density.

Physical Properties Trend

PropertyTrend ↓Reason
Atomic radiusIncreasesExtra electron shells
Melting/Boiling pointDecreases generallyWeaker metallic bonding as atoms get larger
1st Ionisation EnergyDecreasesOuter electrons farther from nucleus
Why Al has a higher melting point than Group 1 & 2 metalsAl has 3 valence electrons contributing to the metallic bond, compared to 1 (Group 1) or 2 (Group 2). More electrons → stronger metallic bond → higher melting point.

Reactions of Aluminium (the most important element)

With Oxygen

4Al(s) + 3O₂(g) → 2Al₂O₃(s)

This protective oxide layer on the surface prevents further corrosion — that is why aluminium "resists corrosion" even though it is reactive.

With Hydrochloric Acid

2Al(s) + 6HCl(aq) → 2AlCl₃(aq) + 3H₂(g) (gas tested with burning splint → 'pop' sound)

With Concentrated H₂SO₄

2Al(s) + 6H₂SO₄(conc.) → Al₂(SO₄)₃(aq) + 3SO₂(g) + 6H₂O(g) (SO₂ decolourises purple KMnO₄ solution)

Note: Al does NOT react with HNO₃ because the Al₂O₃ layer protects it (passivation).

With NaOH (alkali)

2Al(s) + 2NaOH(aq) + 6H₂O(l) → 2NaAl(OH)₄(aq) + 3H₂(g)

This is why aluminium utensils must NOT be washed with strong alkaline solutions — the alkali dissolves the protective oxide layer and then attacks the metal.

With Halogens

2Al(s) + 3Cl₂(g) → 2AlCl₃(s) 2Al(s) + 3F₂(g) → 2AlF₃(s)

Amphoteric Behaviour of Al₂O₃ and Al(OH)₃

Amphoteric = reacts with both acids AND bases. Al₂O₃ is a key example:

Acts as a BASE (with acids) Al₂O₃ + 6H⁺(aq) → 2Al³⁺(aq) + 3H₂O(l)
Acts as an ACID (with bases) Al₂O₃ + 2OH⁻ + 3H₂O → 2[Al(OH)₄]⁻(aq)

Al(OH)₃ (aluminium hydroxide) shows the same behaviour.

Identification of Al³⁺ Ions in Solution

Using NaOH: White precipitate of Al(OH)₃ forms. It dissolves in EXCESS NaOH to give colourless [Al(OH)₄]⁻ complex.
Using NH₃ solution: White precipitate of Al(OH)₃ forms. It does NOT dissolve in excess NH₃ (this distinguishes Al³⁺ from other ions).
Al³⁺(aq) + 3OH⁻(aq) → Al(OH)₃(s) white ppt

Anomalous Behaviour of Boron

Boron is a non-metal, unlike all other Group 13 members. Reasons: small size + high nuclear charge/size ratio + high electronegativity.

PropertyBoron (anomalous)Other Group 13 metals
Electrical conductivityPoor conductorGood conductors
Melting/Boiling pointVery high (2075°C)Much lower
Oxide natureAcidic (B₂O₃)Amphoteric or basic
CompoundsOnly covalentSome ionic compounds
Reaction with dilute acidNo reactionDissolve in acids → H₂ evolved

Inert Pair Effect (Thallium)

Heavier members (Ga, In, Tl) can exhibit the +1 oxidation state in addition to +3. This is the inert pair effect: as you go down the group, the s electrons become more tightly held by the nucleus and less available for bonding. Only the p electron is used → oxidation state +1.

Uses of Group 13 Elements

Aluminium: Cooking utensils, window frames, overhead power cables, aircraft alloys, food packaging, firefighter suits (reflects radiant heat), clay for cement/pots.

Boron: Nuclear reactor control rods (absorbs neutrons), borosilicate glass (test tubes, vacuum flasks), semiconductor additive.

Gallium: Semiconductors, LED (light-emitting diodes).

🧠 The Big Idea for Unit 8
Aluminium is special because it is amphoteric (reacts with both acids and bases) and its protective oxide layer gives it excellent corrosion resistance. Boron is a non-metal and behaves completely differently from the rest of the group.
9
Group 14 Elements & Their Compounds (Carbon Group)
Key competency: Compare chemical properties of Group 14 elements relative to their position in the periodic table

Who Are They?

C (Carbon)Si (Silicon)Ge (Germanium)Sn (Tin)Pb (Lead)

Valence configuration: ns²np² — 4 valence electrons. This group shows the clearest non-metal → metalloid → metal transition. Carbon (non-metal), Si & Ge (metalloids/semiconductors), Sn & Pb (metals).

Physical Properties

PropertyTrend ↓Notes
Atomic radiusIncreasesExtra electron shells
Melting/Boiling pointDecreasesInter-atomic bonds weaken as atoms get larger
DensityIncreasesMass increases faster than volume
ElectronegativityDecreasesLarger radius → less ability to attract
Electrical conductivityGenerally increasesMetallic character increases down group

Carbon — Special Features

Allotropes of Carbon

DiamondEach C bonded to 4 others in a giant tetrahedral structure. Very hard, high melting point. NO mobile electrons → does NOT conduct electricity.
GraphiteEach C bonded to 3 others in hexagonal layers. Layers slide easily → soft, used as lubricant. Delocalised π electrons → CONDUCTS electricity.

Catenation

Carbon's unique ability to form long chains and rings bonded to other carbon atoms (C–C, C=C, C≡C). This is the basis of organic chemistry. Silicon forms Si–O–Si bonds instead of long Si–Si chains.

Oxidation States: +2 and +4

Group 14 elements can form compounds in both +2 and +4 oxidation states. The trend in stability is crucial:

+4 state is more stable at TOPCO₂ is very stable. PbO₂ is unstable and decomposes easily. Stability of +4 state: C > Si > Ge > Sn > Pb
+2 state is more stable at BOTTOMPbO is the most stable Group 14 oxide. CO is unstable (readily oxidised to CO₂). Stability of +2 state: Pb > Sn > Ge > Si > C

The Inert Pair Effect (Ge, Sn, Pb)

As you go down Group 14, the s electrons become more tightly held by the nucleus and less willing to participate in bonding. Only the 2 p electrons are used → oxidation state +2. With a strong oxidising agent, all 4 electrons can be removed → oxidation state +4.

Examples: Pb most commonly forms Pb²⁺ (using p electrons only). PbO₂ (Pb⁴⁺) is unstable and is a powerful oxidising agent.

Reactions of Oxides and Chlorides with Water

CompoundReaction with WaterWhy?
CCl₄Does NOT hydrolyseCarbon has no vacant d-orbitals to accommodate the O atom during reaction
SiCl₄Hydrolyses: SiCl₄ + 2H₂O → SiO₂ + 4HClSilicon has vacant d-orbitals → can form 5-coordinate transition state
SnCl₄Hydrolyses: SnCl₄ + 2H₂O → SnO₂ + 4HClSame reason as Si
CO₂CO₂ + H₂O → H₂CO₃ (weak acid)Acidic oxide; H₂CO₃ does NOT react with acids
SiO₂Does NOT react with waterGiant covalent structure
SiO₂Reacts with HF only: SiO₂ + 4HF → SiF₄ + 2H₂OHF forms stable Si–F bonds
PbO and PbO₂Amphoteric — react with both acids and basesPb is metallic; its oxide shows intermediate character

Thermal Stability of Halides

Thermal stability of tetrahalides decreases down the group: CCl₄ > SiCl₄ > GeCl₄ > SnCl₄ > PbCl₄.

PbCl₄ decomposes readily at room temperature: PbCl₄ → PbCl₂ + Cl₂.

PbBr₄ and PbI₄ do not exist because Br and I are not strong enough oxidising agents to oxidise Pb to +4.

Chemical Tests for Group 14 Ions

IonReagentObservation
Pb²⁺HClWhite precipitate of PbCl₂ (dissolves on heating)
Pb²⁺H₂SBlack precipitate of PbS
Pb²⁺KIYellow precipitate of PbI₂
Pb²⁺OH⁻ (NaOH)White precipitate of Pb(OH)₂, dissolves in excess
Sn²⁺H₂SBrown precipitate of SnS
CO₃²⁻Dilute HClColourless CO₂ gas → turns limewater milky
HCO₃⁻ vs CO₃²⁻MgSO₄ solutionCO₃²⁻ → white precipitate; HCO₃⁻ → no change

Diagonal Relationship (Li/Mg, Be/Al, B/Si)

Pairs of elements diagonally adjacent in periods 2 and 3 show similar properties because the decrease in size going right across a period and increase in size going down a group cancel out, giving similar charge/size ratios.

Diagonal PairKey Similarities
Li / MgBoth form only normal oxides (not peroxides). Li₂CO₃ & MgCO₃ both decompose on heating. Hydroxides decompose on heating. Hydroxides are weak alkalis.
Be / AlBoth oxides (BeO, Al₂O₃) are amphoteric. Both chlorides are covalent. Both rendered passive by conc. HNO₃. Similar atomic radii.
B / SiBoth non-metals with giant covalent structures. Both form weak acids (H₃BO₃, H₂SiO₃). Both have acidic oxides soluble in alkali. Both form hydrides that ignite in air.

Uses of Group 14 Elements

Carbon: Fuel (charcoal/coal), reducing agent in metallurgy, lubricant (graphite), electrodes, pencil leads, diamond in cutting tools & jewellery, radiocarbon dating (C-14).

Silicon: Semiconductors in electronics (transistors, chips), silicates in glass & ceramics, sand in glass production, silicone implants.

Tin: Tin-plating steel cans to prevent corrosion (tinned food cans).

Lead: Lead-acid batteries, radiation shielding (X-rays), lining of sulphuric acid vessels.

Cassiterite (SnO₂) is the tin ore mined in Rwanda.

🧠 The Big Idea for Unit 9
Group 14 shows the most dramatic non-metal → metal transition of any group. The inert pair effect makes the +2 state increasingly stable down the group (especially in Pb). CCl₄ will not hydrolyse (no d-orbitals); SiCl₄ will (has d-orbitals).
10
Group 15 Elements & Their Compounds (Nitrogen Group)
Key competency: Compare properties of Group 15 elements relative to their position in the periodic table

Who Are They?

N (Nitrogen)P (Phosphorus)As (Arsenic)Sb (Antimony)Bi (Bismuth)

Valence configuration: ns²np³ — 5 valence electrons (3 unpaired p electrons). Common oxidation states: +3 and +5. Nitrogen and phosphorus are non-metals; arsenic and antimony are metalloids; bismuth is a metal.

Physical Properties Trend

PropertyTrend ↓Notes
Atomic radiusIncreasesExtra shells; larger atoms
Metallic characterIncreasesN & P: non-metals → As & Sb: metalloids → Bi: metal
1st Ionisation EnergyDecreasesOuter electrons farther from nucleus; easier to remove
ElectronegativityDecreasesLarger radius → less ability to attract electrons
Melting pointIncreases generally (in solids)N is a gas; solid members have higher MP going down

Why Is Nitrogen So Unreactive? (Inertness of N₂)

Nitrogen gas exists as N≡N, a triple bond. The bond energy of N≡N is 942 kJ/mol — one of the strongest bonds in chemistry. Compared to: N–N single bond (247 kJ/mol), O=O double bond (498 kJ/mol).

ConsequenceN₂ is very inert at room temperature. It only reacts at very high temperatures (e.g. lightning, car engines, industrial processes).

Valency of 3 and 5 in Group 15

All Group 15 elements can form 3 bonds (using the 3 unpaired p electrons).
With the exception of nitrogen, they can also form 5 bonds by using vacant d-orbitals (sp³d hybridisation).

Why can't nitrogen form 5 bonds (NCl₅)?Nitrogen has no d-orbitals in its second energy level. It cannot expand its octet. Phosphorus and heavier members CAN expand their octet using empty d-orbitals.
Phosphorus ground state: 1s² 2s² 2p⁶ 3s² 3p³ 3d⁰ After sp³d hybridisation → 5 unpaired electrons available for bonding → PCl₅ can form

Reactions of Group 15 Elements

With Oxygen

N₂ + O₂ → 2NO (at high temperature, e.g. lightning) 2NO + O₂ → 2NO₂ P₄ + 3O₂ → P₄O₆ (limited oxygen → P₂O₃ type) P₄ + 5O₂ → P₄O₁₀ (excess oxygen → P₂O₅ type)

With Hydrogen

N₂(g) + 3H₂(g) ⇌ 2NH₃(g) [Haber Process conditions] All form EH₃ hydrides: NH₃, PH₃, AsH₃, SbH₃, BiH₃

Stability of hydrides decreases down the group: NH₃ most stable → BiH₃ least stable. Basicity also decreases: NH₃ > PH₃ > AsH₃ > SbH₃ > BiH₃.

With Chlorine

P₄ + 6Cl₂ → 4PCl₃ (limited Cl₂) P₄ + 10Cl₂ → 4PCl₅ (excess Cl₂)

With Metals

3Mg + N₂ → Mg₃N₂ (magnesium nitride) 6Li + N₂ → 2Li₃N (lithium nitride)

Ammonia (NH₃) — Laboratory and Industrial

Laboratory Preparation

Method: Heat any ammonium salt with an alkali (e.g. NH₄Cl + Ca(OH)₂).
2NH₄Cl(s) + Ca(OH)₂(s) → CaCl₂ + 2NH₃(g) + 2H₂O Ionic: NH₄⁺ + OH⁻ → NH₃(g) + H₂O(g)

NH₃ is less dense than air → collected by upward delivery. Dried over quicklime (CaO), NOT concentrated H₂SO₄ (it reacts with NH₃).

Industrial Production: Haber Process

N₂(g) + 3H₂(g) ⇌ 2NH₃(g) ΔH = −92 kJ/mol (exothermic)
ConditionValueReason
Temperature450–500°CCompromise: lower T gives better yield but too slow; higher T is faster but very low yield
Pressure200–1000 atmHigh pressure favours the product side (fewer moles of gas)
CatalystFinely divided iron (Fe) + Al₂O₃ promoterIncreases reaction rate without affecting equilibrium position

Chemical Properties of Ammonia

NH₃(g) + H₂O → NH₄⁺(aq) + OH⁻(aq) (weakly alkaline solution) NH₃(g) + HCl(g) → NH₄Cl(s) (white fumes of ammonium chloride) 4NH₃ + 3O₂ → 2N₂ + 6H₂O (burns in O₂, no catalyst) 4NH₃ + 5O₂ → 4NO + 6H₂O (catalytic oxidation — key step in making HNO₃)

Uses of Ammonia

Fertilisers (main use — e.g. ammonium nitrate NH₄NO₃), livestock feed supplement, paper manufacturing, food fermentation, manufacturing of nitric acid.

Nitric Acid (HNO₃) — Laboratory and Industrial

Laboratory Preparation

KNO₃(s) + H₂SO₄(conc.) → KHSO₄(s) + HNO₃(conc.)

Industrial Production: Ostwald Process

Three steps, starting from ammonia:

Step 1: 4NH₃(g) + 5O₂(g) → 4NO(g) + 6H₂O(g) (catalytic chamber, ~600°C, Pt gauze catalyst) Step 2: 2NO(g) + O₂(g) → 2NO₂(g) (cooled to ~50°C in oxidising tower) Step 3: 3NO₂(g) + H₂O(l) → 2HNO₃(l) + NO(g) (absorption tower; NO recycled back)

Reactions of Nitric Acid with Metals

Important rule: HNO₃ is an OXIDISING acid. It almost never produces H₂ with metals (except very dilute HNO₃ with Mg). The reduction product is NO₂ (conc.) or NO (dilute) or N₂O or N₂ or NH₄⁺ (very dilute).
MetalConc. HNO₃Dilute HNO₃
Copper (Cu)Cu + 4HNO₃(conc.) → Cu(NO₃)₂ + 2NO₂ + 2H₂O (brown gas)3Cu + 8HNO₃(dil.) → 3Cu(NO₃)₂ + 2NO + 4H₂O (colourless)
Lead (Pb)Pb + 4HNO₃(conc.) → Pb(NO₃)₂ + 2NO₂ + 2H₂O
Magnesium (Mg)With very dilute (1%): Mg + 2HNO₃ → Mg(NO₃)₂ + H₂
Zinc (Zn)4Zn + 10HNO₃(conc.) → 4Zn(NO₃)₂ + NH₄NO₃ + 3H₂O
Key test: If a sample dissolves in HNO₃ giving a blue solution and brown gas → it is copper, NOT gold (gold does not dissolve in HNO₃).

Reactions with Non-metals (concentrated HNO₃)

C + 4HNO₃(conc.) → CO₂ + 4NO₂ + 2H₂O S + 6HNO₃(conc.) → H₂SO₄ + 6NO₂ + 2H₂O P + 5HNO₃(conc.) → H₃PO₄ + 5NO₂ + H₂O

Uses of Nitric Acid

Production of fertilisers (ammonium nitrate), manufacturing dyes, artificial fibres, drugs, explosives (TNT).

Phosphorus — Key Points

Allotropes of Phosphorus

White Phosphorus (P₄)Waxy solid. Spontaneously ignites in air. Very reactive. Stored under water. Tetrahedral P₄ molecules with 60° bond angles (strained).
Red PhosphorusPolymeric solid. Much less reactive than white phosphorus. Does not ignite spontaneously. Safer to handle. Used in match heads.

Phosphoric Acid (H₃PO₄)

Produced when P₂O₅ reacts with water: P₄O₁₀ + 6H₂O → 4H₃PO₄. A triprotic weak acid with three ionisable H atoms. Used in fertilisers, detergents, rust removal, and food flavouring (cola drinks).

Environmental Impact

Nitrogen oxides (NOₓ) • NO and NO₂ are produced industrially and in car engines.
• Contribute to photochemical smog and acid rain (HNO₃ in rain).
• N₂O (laughing gas) is a potent greenhouse gas.
• Haber process burns fossil fuels → CO₂ → global warming.
• Ostwald process emits NO and NO₂ → must be carefully controlled.
🧠 The Big Picture for Unit 10
N₂ is incredibly unreactive because of its strong triple bond (942 kJ/mol). Once fixed as NH₃ (Haber process), nitrogen becomes enormously useful. HNO₃ is an oxidising acid — it attacks metals by oxidising them (not by releasing H₂). Phosphorus can form 5 bonds (using d-orbitals); nitrogen cannot.